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1.
Ultrason Sonochem ; 105: 106869, 2024 May.
Artigo em Inglês | MEDLINE | ID: mdl-38581797

RESUMO

The level of knowledge on the non-thermal contribution of ultrasonic wave's energy to perform physico-chemical phenomena is one of the bottlenecks for the commercialization purposes. Under constant nominal power of transducer (Pn), the input electrical power (Pin) is less and sensitive to the medium's physical properties. This study attempts to assess the conversion of acoustic to thermal power experimentally and numerically using COMSOL Multiphysis@ for a 24 kHz horn-type sonicator through a medium without any sono-chemical effect. Single- and homogeneous two-phase Newtonian mixtures of sunflower oil and water (o/w) with a relatively wide range of density (914-998 kg/m3) and viscosity (0.5-63.5 mPa.s) were irradiated in a lab-scale vessel (1 L) under batch and continuous flow configuration. The direct influence of Pn (80-400 W) and o/w ratio (0-1) on temperature rise and subsequent thermo-physical properties of liquid and the indirect influence on Pin and thermal energy conversion (TEC) were investigated employing calorimetric method. A new engineering concept including a power factor correlation was proposed and validated for prediction of Pin as a function of liquid space velocity (ϑ), temperature, Prandtl (Pr) and Ohnesorge (Oh) dimensionless groups. The results showed that under constant temperature and Pn, increasing Pr and Oh increased Pin with a similar trend for both modes of operation. An increase in temperature directly led to a decrease in Pin with a power factor closed to "-1". The Pin in continuous flow was higher compared to batch configuration at similar temperature, liquid properties, and Pn. This effect was more significant with increasing ϑ. An increase in ϑ at constant Pn led to a decrease in the inlet/outlet temperature difference in continuous flow and an increase in Pin. Increasing Pn resulted in higher TEC for both configurations; however, TEC was relatively lower in continuous flow than batch configuration indicating more efficient sonication in continuous flow.

2.
Food Sci Nutr ; 12(4): 2334-2345, 2024 Apr.
Artigo em Inglês | MEDLINE | ID: mdl-38628215

RESUMO

By identifying the factors that initiate seed dormancy release, we can reliably predict whether a seed will remain dormant within or exit the seed bank and become a seedling. With regard to annual weed species, assessing which factors efficiently break seed dormancy is critical for estimating the number of weed seeds that will develop into problematic weeds. To better understand dormancy breaking in Redroot pigweed (Amaranthus retroflexus), dormant seeds were treated with cold stratification (4°C for 30 days), application of gibberellic acid (at 500, 1000, 1500, and 2000 parts per million), ultrasound (for 10, 20, 30, and 40 min), soaking in hot water (90°C for 3, 5, 7, and 10 min), and 98% sulfuric acid (for 1, 2, and 3 min). The results showed that Redroot pigweed seed dormancy was effectively broken by cold stratification, gibberellic acid, and ultrasound. Short treatments with hot water had minimal effect while longer times or treatment with sulfuric acid stopped seed germination. In addition to germination percentage, germination rate, plumule length, radicle length, seedling length, seedling dry weight, and seed vigor index were also measured; similarly, application of gibberellic acid had the most significant effect on these parameters. The results of this study add to our knowledge of what processes effectively or ineffectively break Redroot pigweed seed dormancy and promote growth.

3.
Sensors (Basel) ; 24(5)2024 Feb 21.
Artigo em Inglês | MEDLINE | ID: mdl-38474922

RESUMO

Welded lap joints play a vital role in a wide range of engineering structures such as pipelines, storage tanks, pressure vessels, and ship hulls. This study aims to investigate the propagation of ultrasonic guided waves in steel welded lap joints for the baseline-free inspection of joint defects using the mode conversion of Lamb waves. The finite element method was used to simulate a single lap joint with common defects such as corrosion and disbonding. To identify the propagating wave modes, a wavenumber-frequency analysis was conducted using the 2D fast Fourier transform. The power loss of the transmitted modes was also determined to identify damage in the lap joints. The results indicate that the A0 incident in pristine conditions experienced significant transmission losses of about 9.5 dB compared to an attenuation of 2.8 dB for the S0 incident. The presence of corrosion was found to reduce these transmission losses by more than 28%. In contrast, introducing disbonding in the lap joint increased the transmission loss of the S0 incident, while a negligible loss was observed for the A0 incident. The mode-converted S0 (MC-S) and mode-converted A0 (MC-A0) incidents were found to exhibit a unique sensitivity to the presence of corrosion and disbonding. The results indicate that MC-S0 and MC-A0 as well as Lamb mode incidents interact differently in terms of corrosion and disbonding, providing a means to identify damage without relying on baseline signals.

4.
Chempluschem ; 89(5): e202300688, 2024 May.
Artigo em Inglês | MEDLINE | ID: mdl-38199955

RESUMO

With the advancement of scientific research, the introduction of external physical methods not only adds extra freedom to the design of electro-catalytical processes for green technologies but also effectively improves the reactivity of materials. Physical methods can adjust the intrinsic activity of materials and modulate the local environment at the solid-liquid interface. In particular, this approach holds great promise in the field of electrocatalysis. Among them, the ultrasonic waves have shown reasonable control over the preparation of materials and the electrocatalytic process. However, the research on coupling ultrasonic waves and electrocatalysis is still early. The understanding of their mechanisms needs to be more comprehensive and deep enough. Firstly, this article extensively discusses the adhibition of the ultrasonic-assisted preparation of metal-based catalysts and their catalytic performance as electrocatalysts. The obtained metal-based catalysts exhibit improved electrocatalytic performances due to their high surface area and more exposed active sites. Additionally, this article also points out some urgent unresolved issues in the synthesis of materials using ultrasonic waves and the regulation of electrocatalytic performance. Lastly, the challenges and opportunities in this field are discussed, providing new insights for improving the catalytic performance of transition metal-based electrocatalysts.

5.
Chemosphere ; 349: 140832, 2024 Feb.
Artigo em Inglês | MEDLINE | ID: mdl-38042425

RESUMO

Dexamethasone (DXM) is a broadly used drug, which is frequently identified in the water environments due to its improper disposal and incomplete removal in wastewater treatment plant. The inability of conventional treatment processes of wastewater causes that researchers pay a great attention to study and develop effective wastewater treatment systems. This work deals with the study of integrated electro-peroxone/granular activated carbon (EP/US/GAC) process in the degradation of dexamethasone (DXM) from a water environment and the remediation of real pharmaceutical wastewater. Two approaches of response surface methodology based on central composite design (RSM-CCD) and artificial neural network based on algorithm genetic (ANN-GA) were employed for modeling and optimization of the process. Both the models presented significant adequacy for modeling and prediction of the process according to statistical linear and nonlinear metrics (R2 = 0.9998 and 0.9996 and RMSE = 0.2128 and 0.1784 for ANN-GA and RSM-CCD, respectively). The optimization study provided the same outcomes for both ANN-GA and RSM-CCD approaches, where approximately complete DEX oxidation was achieved at pH = 9.3, operating time = 10 min, US power = 300 W/L, applied current = 470 mA, and electrolyte concentration = 0.05 M. A synergistic study signified that the EP/US/GAC process made an 82% synergy index as compared to the individual US and EP processes. The calculated energy consumption for the integrated process was achieved to be 2.79 kW h/gCOD. Quenching test by tert-butanol and p-benzoquinone revealed that HO• radical possessed the largest contribution in DEX degradation. The efficiency of EP/US/GAC process in the remediation of real pharmaceutical wastewater showed a significant decline in COD content (92% removal after 180 min), and the ratio of initial BOD/COD ratio of 0.27 was elevated up to 0.7 after 100 min treatment time. The performance stability of EP/US/GAC system showed no remarkable drop in removal efficiency, and leakage of lead ions from the anode surface was negligible and below WHO guideline for drinking water. Generally, this research work manifested that the integrated EP/US/GAC system elevated the degradation efficiency and can be proposed as a pretreatment step before biological treatment processes for the remediation of recalcitrant wastewaters.


Assuntos
Águas Residuárias , Poluentes Químicos da Água , Carvão Vegetal/química , Poluentes Químicos da Água/química , Redes Neurais de Computação , Preparações Farmacêuticas , Dexametasona , Água
6.
Curr Org Synth ; 21(2): 127-139, 2024.
Artigo | MEDLINE | ID: mdl-36998127

RESUMO

"The founder of green chemistry explains how chemicals manufacturing must change to support a sustainable future." In this review, Green chemistry is considered in the synthesis of heterocycles compounds containing Pyrimidine nuclei using different catalyzes, solvents, and techniques for the synthesis of pyrimidine derivatives that achieve sustainability. The mentioned fused heterocycles are classified according to the type of ring system. The yield of the target molecules reported in the review is given in the reaction's last step.

7.
J Microsc ; 292(2): 90-102, 2023 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-37698414

RESUMO

Scanning acoustic microscopy (SAM) is a potent and nondestructive technique capable of producing three-dimensional topographic and tomographic images of specimens. This is achieved by measuring the differences in time of flight (ToF) of acoustic signals emitted from various regions of the sample. The measurement accuracy of SAM strongly depends on the ToF measurement, which is affected by tilt in either the scanning stage or the sample stage. Hence, compensating for the ToF shift resulting from sample tilt is imperative for obtaining precise topographic and tomographic profiles of the samples in a SAM. In the present work, we propose an automated tilt compensation in ToF of acoustic signal based on proposed curve fitting method. Unlike the conventional method, the proposed approach does not demand manually choosing three separate coordinate points from SAM's time domain data. The effectiveness of the proposed curve fitting method is demonstrated by compensating time shifts in ToF data of a coin due to the presence of tilt. The method is implemented for the correction of different amounts of tilt in the coin corresponding to angles 6.67°, 12.65° and 15.95°. It is observed that the present method can perform time offset correction in the time domain data of SAM with an accuracy of 45 arcsec. The experimental results confirm the effectiveness of the suggested tilt compensation technique in SAM, indicating its potential for future applications.

8.
J Arthropod Borne Dis ; 17(1): 83-93, 2023 Mar.
Artigo em Inglês | MEDLINE | ID: mdl-37609562

RESUMO

Background: The German cockroach, Blattella germanica (Insecta: Blattodea, Blattellidae), which occurs widely in human buildings, is a small cockroach species. Cockroach control chemical pesticides are toxic to the environment, and it is sometimes impossible to prevent them. Controlling Blattella germanica through ultrasonic waves can be efficient and less dangerous for the environment. Methods: In this study, the repellency and lethal effect of ultrasonic waves on male and female German cockroaches was tested in a twin glass cubic chamber at laboratory condition. The wave frequencies tested ranged from 20 to 100kHz with 5kHz steps. A signal generator generated these frequencies, and the piezoelectric transmitter of these ultrasonic waves was positioned in the chamber's center on the upper side. Results: Fisher's test showed that there was the greatest repellency effect in both male and female at frequencies of 35 and 40kHz. According to the results of the regression test, the most lethal effect is at the frequencies of 40 and 75kHz. Conclusion: The operating ultrasonic frequencies investigated in this study can be used to repel and kill German cockroaches as pests endangering human health and environment.

9.
Trials ; 24(1): 389, 2023 Jun 09.
Artigo em Inglês | MEDLINE | ID: mdl-37296443

RESUMO

BACKGROUND: Viral pneumonia has always been a problem faced by clinicians because of its insidious onset, strong infectivity, and lack of effective drugs. Patients with advanced age or underlying diseases may experience more severe symptoms and are prone to severe ventilation dysfunction. Reducing pulmonary inflammation and improving clinical symptoms is the focus of current treatment. Low-intensity pulsed ultrasound (LIPUS) can mitigate inflammation and inhibit edema formation. We aimed to investigate the efficacy of therapeutic LIPUS in improving lung inflammation in hospitalized patients with viral pneumonia. METHODS: Sixty eligible participants with clinically confirmed viral pneumonia will be assigned to either (1) intervention group (LIPUS stimulus), (2) control group (null stimulus), or (3) self-control group (LIPUS stimulated areas versus non-stimulated areas). The primary outcome will be the difference in the extent of absorption and dissipation of lung inflammation on computed tomography. Secondary outcomes include changes in lung inflammation on ultrasonography images, pulmonary function, blood gas analysis, fingertip arterial oxygen saturation, serum inflammatory factor levels, the sputum excretion volume, time to the disappearance of pulmonary rales, pneumonia status score, and course of pneumonia. Adverse events will be recorded. DISCUSSION: This study is the first clinical study of the efficacy of therapeutic LIPUS in the treatment of viral pneumonia. Given that the current clinical recovery mainly depends on the body's self-limiting and conventional symptomatic treatment, LIPUS, as a new therapy method, might be a major advance in the treatment of viral pneumonia. TRIAL REGISTRATION: ChiCTR2200059550 Chinese Clinical Trial Registry, May 3, 2022.


Assuntos
COVID-19 , Pneumonia Viral , Humanos , SARS-CoV-2 , Pneumonia Viral/tratamento farmacológico , Inflamação , Ondas Ultrassônicas , Resultado do Tratamento , Ensaios Clínicos Controlados Aleatórios como Assunto
10.
Front Neurol ; 14: 1157335, 2023.
Artigo em Inglês | MEDLINE | ID: mdl-37332988

RESUMO

Objective: The outcomes of physical therapy are commonly assessed with subjective scales and questionnaires. Hence, a continuous search to identify diagnostic tests that would facilitate objective assessment of symptom reduction in those patients with Achilles tendinopathy who undergo mechanotherapy. The main aim of this study was to evaluate and compare the effectiveness of shock wave and ultrasound treatments, using objective posturographic assessment during step-up and step-down initiation. Materials and methods: The patients with non-insertional Achilles tendinopathy and pain lasting for more than 3 months were randomly assigned to one of the experimental groups, i.e., radial shock wave therapy (RSWT), ultrasound therapy, or placebo ultrasound. All groups also received deep friction massage as the primary therapy. The transitional locomotor task was performed with the affected and unaffected limb in random order, on two force platforms under two conditions (step-up and step-down). The recording of center of foot pressure displacements was divided into three phases: quiet standing before step-up/step-down, transit, and quiet standing until measurement completion. Pre-intervention measurements were performed and then short-term follow-ups at weeks 1 and 6 post-therapy. Results: The three-way repeated measures ANOVA showed few statistically significant two-factor interactions between therapy type, time point of measurement and the type of the locomotor task. Significant increases in postural sway were observed in the entire study population throughout the follow-up period. Three-way ANOVAs revealed a group effect (shock wave vs. ultrasound) on almost all variables of the quiet standing phase prior to step-up/step-down initiation. Overall, postural stability before the step-up and step-down tasks appeared to be more efficient in patients who had undergone RSWT compared to the ultrasound group. Conclusion: Objective posturographic assessment during step-up and step-down initiation did not demonstrate therapeutic superiority of any of the three therapeutic interventions used in patients with non-insertional Achilles tendinopathy.Clinical Trial Registration: The trial was prospectively registered in the Australian and New Zealand Clinical Trials Registry (no. ACTRN12617000860369; registration date: 9.06.2017).

11.
Ultrasonics ; 128: 106866, 2023 Feb.
Artigo em Inglês | MEDLINE | ID: mdl-36283263

RESUMO

The characteristics of the heat transfer and friction loss of turbulent water flow in a circular pipe were investigated experimentally at a constant surface temperature of 45 ℃ for 28 kHz ultrasound propagation along the mainstream flow. Transducers were installed in five rows and three columns in the upstream section of the test pipe, and the number of active transducers was varied (1, 3, and 15) for a Reynolds number range of 10,000-25,000. The results indicated that the ultrasonic effects yielded positive results for both the heat transfer and pressure loss of the pipe flow. Under the influence of 15 ultrasonic transducers, the maximum Nusselt number ratio was 1.57 and the greatest reduction in the friction factor was 21.6 % for a Reynolds number of 10,000. The corresponding maximum thermal performance factor was approximately 1.7. However, the thermal efficiency tended to decrease with an increase in the number of transducers. The maximum thermal efficiency values under ultrasonic waves with 1, 3, and 15 transducers were 5.43, 3.37, and 1.95, respectively. When the change in the friction factor per ultrasonic input power was considered, the most suitable number of ultrasonic transducers was three. Finally, predictive formulas were proposed for the Nusselt number ratio and friction factor ratio under low-frequency ultrasound, with deviations from -5.5 % to 5.4 % and -7.4 % to 7.4 %, respectively.

12.
Clin Biomech (Bristol, Avon) ; 101: 105830, 2023 01.
Artigo em Inglês | MEDLINE | ID: mdl-36469960

RESUMO

BACKGROUND: The troublesome symptoms of Achilles tendinopathy prompt patients to seek effective forms of conservative treatment. The main aim of the study was to determine the therapeutic efficacy of shock wave and ultrasound therapies for Achilles tendinopathy in reducing pain intensity. Treatment efficacy was also assessed using objective posturographic measurements. METHODS: Thirty-nine patients patients were randomly allocated to one of three experimental groups that received shock wave therapy (group A), ultrasound therapy (group B) and placebo ultrasound (group C). Posturographic measurements and subjective assessment of pain intensity were taken prior to therapy and at weeks 1 and 6 of therapy completion. FINDINGS: A comparison of percentage change in activity-related pain from baseline to 6 weeks post-therapy revealed a significantly greater pain reduction in group A compared to group B. The three-way ANOVA demonstated an effect of treatment type on all posturographic variables. The Bonferroni post-hoc test showed the means of all variables were significantly smaller for group A than group B. Limb condition also had an effect on the center-of-pressure trajectories in anteroposterior plane; the post-hoc test showed the mean values of the variables were significantly greater for the non-affected compared to affected limb. INTERPRETATION: Shock wave therapy was significantly more effective than sonotherapy for alleviation of activity-related pain of Achilles tendinopathy. An association was also shown between shock wave therapy and more efficient postural control in patients with Achilles tendinopathy. The parameters of center-of-pressure trajectories in the sagittal plane were significantly greater for the non-affected compared to affected limb. The trial was prospectively registered in the Australian and New Zealand Clinical Trials Registry (no. ACTRN12617000860369; registration date: 9.06.2017).


Assuntos
Tendão do Calcâneo , Tratamento por Ondas de Choque Extracorpóreas , Tendinopatia , Humanos , Medição da Dor , Tendinopatia/terapia , Austrália , Dor , Resultado do Tratamento
13.
J Hepatobiliary Pancreat Sci ; 30(3): 351-359, 2023 Mar.
Artigo em Inglês | MEDLINE | ID: mdl-35918909

RESUMO

BACKGROUND/PURPOSE: Shear wave elastography (SWE) is a clinical method used to evaluate liver hardness. In this study, we assessed its applicability in assessing the pancreas and its potential for diagnosing chronic pancreatitis. METHODS: We performed SWE on 59 patients who underwent abdominal ultrasound, and measured the computed tomography (CT) values of the pancreas. Patients were classified as having a normal pancreas (NP), early chronic pancreatitis (ECP), or chronic pancreatitis (CP). SW elasticity (SWe), SW dispersion (SWd), and CT values between groups were analyzed. RESULTS: SWe significantly differed between the CP and NP/ECP groups (NP vs CP; P = 0.001, ECP vs CP; P = 0.026,), while SWd showed a significant difference only between the NP and CP group (NP vs CP; P = 0.001). The CT values were significantly different between the CP and NP/ECP groups (NP vs CP; P = 0.0006, ECP vs CP; P = 0.0027). CONCLUSION: Pancreatic SWE and CT values were helpful in the diagnosis of chronic pancreatitis. SWd may reveal status changes in ECP.


Assuntos
Técnicas de Imagem por Elasticidade , Pancreatite Crônica , Humanos , Técnicas de Imagem por Elasticidade/métodos , Pancreatite Crônica/diagnóstico por imagem , Pâncreas/diagnóstico por imagem , Ultrassonografia , Fígado
14.
Acta cir. bras ; 38: e380023, 2023. tab, graf, ilus
Artigo em Inglês | LILACS, VETINDEX | ID: biblio-1419864

RESUMO

Purpose: Low-intensity pulsed ultrasound (LIPUS) has been used to stimulate the healing of the fresh fracture, delayed union, and non-union in both animal and clinical studies. Besides, biphasic calcium phosphate ceramic (BCP) is a promising biomaterial for bone repair as it shows favorable biocompatibility, osteoinduction, and osteoconduction. However, scarcity is known about the combined effect of LIPUS and BCP on bone formation. Methods: The combined effect of LIPUS and BCP was studied in a beagle model. Twelve dogs were used. BCP granules without any additions were implanted into bilateral erector spinae muscles. One side is the BCP group, while the counterlateral side is LIPUS + BCP group. Histological and histomorphometric analyses, and quantitative real-time polymerase chain reaction were evaluated. Results: Compared with BCP alone, the LIPUS + BCP showed no advantages in early bone formation. Furthermore, the Notch signaling pathway-related mRNA has no significant difference between the two groups. Conclusions: The preliminary results showed that the BCP, which has intrinsic osteoinduction nature, was an effective and promising material. However, LIPUS has no enhanced effect in BCP induced ectopic bone formation. Furthermore, LIPUS has no effect on the Notch signaling pathway. Whether costly LIPUS could be used in combination with BCP should be a rethink.


Assuntos
Animais , Cães , Osteogênese/fisiologia , Terapia por Ultrassom/veterinária , Materiais Biocompatíveis , Cerâmica/análise
15.
Materials (Basel) ; 15(19)2022 Sep 29.
Artigo em Inglês | MEDLINE | ID: mdl-36234093

RESUMO

Structural health monitoring systems for composite laminates using guided ultrasonic waves become more versatile with the structural integration of sensors. However, the data generated within these sensors have to be transmitted from the laminate to the outside, where polyimide-based printed circuit boards play a major role. This study investigates, to what extent integrated polyimide inlays with applied sensor bodies influence the guided ultrasonic wave propagation in glass fiber-reinforced polymer specimens. For reasons of resource efficiency, narrow specimens are used. Numerical simulations of a damping-free specimen indicate reflections of the S0-mode at the integrated inlay. This is validated experimentally with an air-coupled ultrasonic technique and a 3D laser Doppler vibrometry measurement. The experimental data are evaluated with a method including temporal and spatial continuous wavelet transformations to clearly identify periodically occurring wave packages as edge reflections and distinguish them from possible inlay reflections. However, even when separating in-plane and out-of-plane movements using the 3D measurement, no reflections at the inlays are detected. This leads to the conclusion that polyimide inlays are well suited as substrates for printed circuit boards integrated into fiber-reinforced polymer structures for structural health monitoring, since they do not significantly influence the wave propagation.

16.
Molecules ; 27(19)2022 Sep 24.
Artigo em Inglês | MEDLINE | ID: mdl-36234843

RESUMO

High concentrations of antibiotics have been identified in aqueous media, which has diminished the quality of water resources. These compounds are usually highly toxic and have low biodegradability, and there have been reports about their mutagenic or carcinogenic effects. The aim of this study was to apply zero-valent iron-oxide nanoparticles in the presence of hydrogen peroxide and the sonolysis process for the removal of the amoxicillin antibiotic from aqueous media. In this study, zero-valent iron nanoparticles were prepared by an iron chloride reduction method in the presence of sodium borohydride (NaBH4), and the obtained nanoparticles were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and vibrating-sample magnetometry (VSM). Then, using a Fenton-like process, synthetic wastewater containing 100 to 500 mg/L amoxicillin antibiotic was investigated, and the effects of different parameters, such as the frequency (1 and 2 kHz), contact time (15 to 120 min), the concentration of hydrogen peroxide (0.3%, 0.5%, and 6%), the dose of zero-valent iron nanoparticles (0.05, 0.1, 0.5 g/L), and pH (3, 5, 10) were thoroughly studied. A pH of 3, hydrogen peroxide concentration of 3%, ultrasonic-wave frequency of 130 kHz, zero-valent iron nanoparticles of 0.5 g/L, and contaminant concentration of 100 mg/L were obtained as the optimal conditions of the combined US/H2O2/nZVI process. Under the optimal conditions of the combined process of zero-valent iron nanoparticles and hydrogen peroxide in the presence of ultrasonic waves, a 99.7% removal efficiency of amoxicillin was achieved in 120 min. The results show that the combined US/H2O2/nZVI process could be successfully used to remove environmental contaminants, including antibiotics such as amoxicillin, with a high removal percentage.


Assuntos
Nanopartículas , Poluentes Químicos da Água , Amoxicilina , Antibacterianos , Cloretos , Peróxido de Hidrogênio/química , Ferro/química , Águas Residuárias/química , Água , Poluentes Químicos da Água/química
17.
Sensors (Basel) ; 22(18)2022 Sep 14.
Artigo em Inglês | MEDLINE | ID: mdl-36146311

RESUMO

Commercially available photopolymer resins can be combined with lead zirconate titanate (PZT) micrometer size piezoelectric particles to form 3D-printable suspensions that solidify under UV light. This in turn makes it possible to realize various non-standard sensor geometries which might bring benefits, such as increased piezoelectric output in specific conditions and less interference with incoming waves due to better acoustical adaptation compared to solid PZT ceramics. However, it is unclear whether piezoelectric composite materials are suitable for guided ultrasonic wave (GUW) detection, which is crucial for structural health monitoring (SHM) in different applications. In this study, thin piezoelectric composite sensors are tape casted, solidified under UV light, covered with electrodes, polarized in a high electric field and adhesively bonded onto an isotropic aluminum waveguide. This approach helps to demonstrate the capabilities of tape casting's freedom to manufacture geometrically differently shaped, thin piezoelectric composite sensors for GUW detection. In an experimental study, thin two-dimensional piezoelectric composite sensors demonstrate successful detection of GUW for frequency-thickness products of up to 0.5 MHz mm. An analytical calculation of the maximum and minimum amplitudes for the ratio of the wavelength and the sensor length in wave propagation direction shows good agreement with the sensor-recorded signals. The output of the piezoelectric composite sensors and occurring reflections as measure for wave interactions are compared to commercial piezoelectric discs to evaluate their performance.


Assuntos
Alumínio , Transdutores , Cerâmica/química , Eletrodos , Ondas Ultrassônicas
18.
Sensors (Basel) ; 22(14)2022 Jul 19.
Artigo em Inglês | MEDLINE | ID: mdl-35891047

RESUMO

Structural health monitoring of lightweight constructions made of composite materials can be performed using guided ultrasonic waves. If modern fiber metal laminates are used, this requires integrated sensors that can record the inner displacement oscillations caused by the propagating guided ultrasonic waves. Therefore, we developed a robust MEMS vibrometer that can be integrated while maintaining the structural and functional compliance of the laminate. This vibrometer is directly sensitive to the high-frequency displacements from structure-borne ultrasound when excited in a frequency range between its first and second eigenfrequency. The vibrometer is mostly realized by processes earlier developed for a pressure sensor but with additional femtosecond laser ablation and encapsulation. The piezoresistive transducer, made from silicon, is encapsulated between top and bottom glass lids. The eigenfrequencies are experimentally determined using an optical micro vibrometer setup. The MEMS vibrometer functionality and usability for structural health monitoring are demonstrated on a customized test rig by recording application-relevant guided ultrasonic wave packages with a central frequency of 100 kHz at a distance of 0.2 m from the exciting ultrasound transducer.


Assuntos
Sistemas Microeletromecânicos , Lasers , Transdutores , Ondas Ultrassônicas , Ultrassonografia
19.
Sensors (Basel) ; 22(7)2022 Mar 24.
Artigo em Inglês | MEDLINE | ID: mdl-35408118

RESUMO

Damage detection of railway tracks is vital to ensure normal operation and safety of the rail transit system. Piezoelectric sensors, which are widely utilized to receive ultrasonic wave, may be disturbed in the railway system due to strong electromagnetic interference (EMI). In this work, a hybrid ultrasonic sensing system is proposed and validated by utilizing a lead-zirconate-titanate (PZT) actuator and a fiber Bragg grating (FBG) sensor to evaluate damage conditions of the railway tracks. The conventional ultrasonic guided wave-based method utilizing direct wave to detect damages is limited by the complex data analysis procedure and low sensitivity to incipient damage. Diffuse ultrasonic wave (DUW), referring to later arrival wave packets, is chosen in this study to evaluate structural conditions of railway tracks due to its high sensitivity, wider sensing range, and easy implementation. Damages with different sizes and locations are introduced on the railway track to validate the sensitivity and sensing range of the proposed method. Two damage indices are defined from the perspective of energy attenuation and waveform distortion. The experimental results demonstrate that the DUW signals received by the hybrid sensing system could be used for damage detection of the railway tracks and the waveform-distortion-based index is more efficient than the energy-based index.


Assuntos
Ondas Ultrassônicas , Ultrassom
20.
Front Plant Sci ; 13: 833858, 2022.
Artigo em Inglês | MEDLINE | ID: mdl-35419018

RESUMO

Soybean seeds contain substantial triacylglycerols and fatty acids that are prone to oxidation during storage, contributing to the dramatic deterioration of seed vigor. This study reports an ultrasonic waves treatment (UWT), which is a physical method capable of promoting the germination ability of the aged soybean seeds by regulating the antioxidant defense and gluconeogenesis. Germination test revealed that UWT significantly increased the germination rate and seedlings' establishment of the soybean seeds stored for 12 months, although insignificantly impacting the vigor of fresh (stored for 1 month) and short-term stored (for 6 months) seeds. Further biochemical analysis revealed that UWT decreased the hydrogen peroxide (H2O2), O2⋅-, and malondialdehyde contents in the aged soybean seeds during early germination. Consistently, UWT prominently elevated the activities of superoxide dismutase, catalase, and acetaldehyde dehydrogenase, and also the corresponding gene expressions. Besides, the soluble sugar content of UWT was significantly higher than that of the untreated aged seeds. Analysis of enzyme activity showed UWT significantly upregulated the activities of several key enzymes in gluconeogenesis and the transcription levels of corresponding genes. Moreover, UWT enhanced the invertase activity within aged seeds, which was responsible for catalyzing sucrose hydrolysis for forming glucose and fructose. In summary, UWT improved germination and seedlings establishment of aged soybean seeds by regulating antioxidant defense and gluconeogenesis. This study expands the application of ultrasonication in agricultural production and further clarifies the physiological and molecular mechanisms of the aged seed germination, aiming to provide theoretical and practical guidance for seed quality and safety.

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